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N15 NMR

September 23 @ 1:00 pm - 3:00 pm EDT

In September 2021 IVAN will host a N15 NMR workshop. Actual Date still to be determined.

Nitrogen is ubiquitous, incorporated in small molecule natural products, pharmaceutical agents, and pharmacologically active peptides.  15N, the spin 1/2 isotope of nitrogen amenable to NMR observation, is notoriously challenging for direct observation with low natural abundance (0.37%) and, relatively speaking, a low observation frequency roughly 10% of the 1H NMR observation frequency on a given NMR instrument with experiments further exacerbated by a negative nOe.  Nonetheless, beginning in the early 90’s, it became feasible to perform both one-bond and long-range 1H-15N heteronuclear shift correlation experiments on small samples.  The panel discussion will address experiment choices and optimization as well as utilizing 15N NMR data in structure elucidation studies.

Details

Date:
September 23
Time:
1:00 pm - 3:00 pm EDT

Venue

IVAN Users Group Zoom Online Workshop
160 Authority Drive
FItchburg, MA 01420 United States

Organizers

IVAN Users Group
MR Resources
Q.One Americas